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Effect of salt on pores (benchtop)
(Transferred from old blog) The above TEM images show that RTP (800C, 5 min) treated samples (from W334) have their pores intact in salt over a period of time! 1M and 2M NaCl solutions were used and TEM samples were taken at different time points. There is some deformation observed near the edges of the…
Continued analysis of SiN-NP permeance and permeability
Following up on our previous work with SiN-NP with varied RIE times, Sarah and I measured permeability and permeance using a new measuring system better suited to the higher permeance and permeability we expect with the larger pores and higher porosity. Using the pressure regulator pictured above, we can set pressures of 3 psi and above…
Fluidics and cultured cells on pnc-Si
As a proof-of-principle, Henry and I have been working on a microfluidic device for flowing blood cells/particles across cultured cells on pnc-Si. More on why this is important later. We’ve come up with a prototype and I’ve been testing it out. I will include schematics later but here are the first couple of movies I’ve…
Process Variables to imitate wafer 1085 npMgF2/npAu
Summary I want to imitate the material properties from 1085 as they have given us the best SERS performance to date. We have the best information that we’ve ever had before imitating the nanostructure and nanotopology from the MgF2. Our belief is that getting infilled Au close together in a nanopore dramatically enhances the electric…
30 nm pnc-Si bias series
We have already established that bias is an important parameter in controlling the morphology of 15 nm thick pnc-Si, but have yet to look at its effect on thicker films. This week, made a few 30 nm thick Si films with 02, 05, 25, and 50 W of substrate bias. I annealed these films at…
pinhole-less membranes
Inspired by JP, we decided to try to etch amorphous (unannealed) wafers this week to see if pinhole density changed. To my surprise, the amorphous membranes had no pinholes! Furthermore, I tried to anneal the membranes after the etch and they went flat indicating crystallization! Refer to the table below for the results. Wafer 565:…
