Updated: 25-40-25 nm OSO SEPCONS
We created a 25-40-25 OSO stack with a SEPCON pattern. RTP at 1050 C 100 C/s 60 s. The following images show a comparison between the STEM detector and the SEM detector, and then a couple more images at 100 kx and 50 kx.





I calculated a porosity of ~6.5 %, and avg. pore diameter of ~40 nm.
I measured a permeance of ~500 cc/cm2/s/bar and burst pressures of 1.2, 11.2, 20.2, 19.3, 21.1 psi.
Only about 50-60 % of the wafers chips were in tact after etching. That is surprising given the relatively high burst pressures I measured. The majority of broken membranes were located in the same region of the wafer.

I updated the post. Now there are histograms of pore sizes as well as a comparison of the SEM and STEM image porosity and avg. dia.