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This is great news! The image is fascinating- there is no clear evidence for this amorphous phase here- and the apparent shape of the nanocrystals is very interesting- not at all spherical, it seems! Do you have more of these pictures? I think they can give us important clues on how the pores form.
Is the low throughput due to inexperience with the tool or is it the nature of the tool?
I agree, this material is highly crystalline. (On a similar note, Brian said that we need to be within +/- 0.5 degrees of the Bragg condition to see diffracting crystals.) I was only able to look at one sample today because it was the first time I touched the tool and we were being trained.
Throughput is limited on this TEM because you can only load one sample at a time (vs. two w/ Karen’s) and the pump time is significantly longer because of the higher vacuum requirement.