An important result of last weeks experiment showed that Antimony (Sb) doped substrates had no pinhole defects; however, Phosphorous doped substrates from the same batch had many very small pinholes. This agrees with a previous experiment: Antimony wafers have shown no pinhole formation. I propose a model that aims to explain:1) Why we are not…
This week’s production included wafers of antimony (Sb) and phosphorus (P) doping. Process parameters The deposition heater was re-brazed prior to this deposition. We were concerned with the original brazing job because there were areas with “globs” of material and cracks in the solder. The new braze covers most of the surface, and although is…
Process Summary for the week of 12/3 -12/10/2007: Simpore Process Flow.xls JP
I reran a set of hydraulic permeability tests at 16.56psi (3500RPM) hoping that this would clarify the previously collected data at the 21.63psi (4000RPM) and the 33.79psi (5000RPM) range that did not seem to agree with the trend of the other data points. As shown above this point still does not seem to be in…
We have previously discussed how the membranes near the center of the wafer have very small pores, while as you progress outward larger pores begin to appear. I tested one of these central membranes from wafer 304 (TEM sample, position -1,0) using our standard fluorescence microscope based assay. I observed obvious rhodamine diffusion through this…
I took a closer look at some of Lingyun’s samples today, and captured some interesting TEM images. wafer 205 with 10 nm Ti @ 35kx wafer 205 with 10nm Ti @ 250kx wafer 205 with 10nm Ti & 10nm Au @ 35kx wafer 205 with 10nm Ti & 10nm Au @ 200kx The higher mag….
Surface functionalization results
The graph below shows the burst pressures for302, 303, 304, 307 wafers.
The objective of last week’s production was to track down the source of Cu contamination. The good news is that none of the wafers showed signs of Cu. The bad news is we are not sure why it has disappeared all of the sudden. Chris and I observed that there are particles in the well…
UPDATED 12/12/07 – Added data on albumin. In these gels, the band from beta-galactosidase appears to overlap with phosphorylase b making it difficult to determine which protein passes and which is retained. I have used Mike Bindschadler’s pore imaging software to find the pore sizes of the three membranes I have use to perform succesful…