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Permeance tests with new Omega rotameter

Yaron has acquired an Omega rotameter (FL-3803ST) with interchangeable flow tubes.  The tubes operate in three different ranges low (6-61 mL/min, 042-15-N), medium (150-1,682 mL/min, 082-03-N), and High (1,000-23,752 mL/min, 034-39-N).  I’ve attached an excel file with the calibration data plotted.  We fit the curves with polynomial trendline to get equations.  Also in the workbook below is a sheet where you input the reading and get the flow rate from each tube using the equations.

Omega_rotameter_calibrations

To measure the permeance, we used the following setup:  Nitrogen tank->pressure regulator-> VWR digital manometer-> rotameter->sample->atmosphere.  We measured some 5-slot NPN and pnc-Si samples for the NPN manuscript and here are the results:

30s etch 6.5% 22%porosity, 56nm pores- 61,000 ml/min/cm2/bar

40s etch 38% porosity, 78nm pores- 181,000 ml/min/cm2/bar

30nm pnc-si (wafer 1038) 9.5% porosity, 37nm pores- 30,000 ml/min/cm2/bar

40nm pnc-si 6.5% porosity, 40nm pores-  25,000 ml/min/cm2/bar

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